Asynt ReactoMate CLR Reaction Systems

ReactoMate Reaction Systems
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Description

The ReactoMate laboratory and ReactoMate-Pilot reaction systems offers precise control of reaction variables, a powerful direct drive overhead stirrer and excellent reaction visibility with the vacuum jacket option.

The ReactoMate CLR reaction systems are fully customisable to the users requirements with an extensive range of options.  Just as an example, we would offer a PTFE lid with a variety of ports/fittings as standard but we can make a custom lid to suit your specific needs from PTFE or glass.  The flange can be altered to suit, as well as side arms and valves, of course, as just a few things that can be customised at your request.

One of the problematic issues associated with reaction vessel set up is the cumbersome and, often dangerous, scaffolding supporting the unit. Support frames often have bars at the front and sides this can lead to problematic access to reactor and potential fracturing of glassware if exchanging vessels.

The ReactoMate-Pilot Super Support (RSS) system from Asynt provides a simple, straightforward and easy way to support your jacketed reactor any size up to 30,000 ml. Made from highly chemical resistant materials the RSS makes access to your reactor much more manageable. With a compact footprint and lifting mechanism (Easy raising/lowering of vessels with one hand, even 30,000 ml!) it makes it an excellent space saver in the fumehood. Contact us to arrange a demo in your laboratory.

To make it easy to get up and running from scratch with a ReactoMate-Pilot we are now offering packages including everything you need.

To complement the ReactoMate Controlled Lab Reactor products, we offer a wide choice of compatible circulators from the several manufacturers, including theJulabo range.  The Julabo CF41 for example will cool a 1L reaction in a ReactoMate single jacketed vessel down to -20oC.

In addition, we have partnered with Mettler Toledo to offer the RX-10 full automation for your ReactoMate allowing you to program thermostat temperature, liquid dosing and sampling, and integrating process analytical technology for data rich experiments, day or night.

Our team of experts will work in close cooperation with you to ensure that you get the exact product required, to the highest standard.

Find out more about how Innovative Physical Organic Solutions (IPOS), consultants in the  complexities associated with optimising and scaling-up laboratory processes

 

 

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The ReactoMate laboratory and ReactoMate-Pilot reaction systems offers precise control of reaction variables, a powerful direct drive overhead stirrer and excellent reaction visibility with the vacuum jacket option.

The ReactoMate CLR reaction systems are fully customisable to the users requirements with an extensive range of options.  Just as an example, we would offer a PTFE lid with a variety of ports/fittings as standard but we can make a custom lid to suit your specific needs from PTFE or glass.  The flange can be altered to suit, as well as side arms and valves, of course, as just a few things that can be customised at your request.

One of the problematic issues associated with reaction vessel set up is the cumbersome and, often dangerous, scaffolding supporting the unit. Support frames often have bars at the front and sides this can lead to problematic access to reactor and potential fracturing of glassware if exchanging vessels.

The ReactoMate-Pilot Super Support (RSS) system from Asynt provides a simple, straightforward and easy way to support your jacketed reactor any size up to 30,000 ml. Made from highly chemical resistant materials the RSS makes access to your reactor much more manageable. With a compact footprint and lifting mechanism (Easy raising/lowering of vessels with one hand, even 30,000 ml!) it makes it an excellent space saver in the fumehood. Contact us to arrange a demo in your laboratory.

To make it easy to get up and running from scratch with a ReactoMate-Pilot we are now offering packages including everything you need.

To complement the ReactoMate Controlled Lab Reactor products, we offer a wide choice of compatible circulators from the several manufacturers, including theJulabo range.  The Julabo CF41 for example will cool a 1L reaction in a ReactoMate single jacketed vessel down to -20oC.

In addition, we have partnered with Mettler Toledo to offer the RX-10 full automation for your ReactoMate allowing you to program thermostat temperature, liquid dosing and sampling, and integrating process analytical technology for data rich experiments, day or night.

Our team of experts will work in close cooperation with you to ensure that you get the exact product required, to the highest standard.

Find out more about how Innovative Physical Organic Solutions (IPOS), consultants in the  complexities associated with optimising and scaling-up laboratory processes

 

 

Single jacketed reaction vessel with Zero Dead Space bottom drain valve (vessel can be linked to a suitable heater/chiller) up to 50,000 ml

PTFE multi neck reaction lid as standard with all kits

Simple upgrade option to change PTFE lid for a custom glass lid.

Standard (for any size vessel), Datum (vessels up to 5L) and Super Support Systems (vessels to 30L)

Custom Options are available

Vacuum jacketed vessels to 10,000 ml

Read our press release: “Higher Performance from vacuum jacketed reactor system”

PhosphonicS: Asynt has been working with the chemists at PhosphonicS on “Effective Scale-up of Functionalised Silicas” – click Asynt PR 17-07-12 ReactoMate for the associated press release.

Asynt PR – Higher Performance from vacuum jacketed reactor system
Asynt ReactoMate CLR systems brochure

Asynt work closely with IPOS to provide essential tools and know-how for efficient process understanding and optimisation. Several such factors are assessing how various types of agitator, the size and shape of the reactor and the addition of baffles affect mixing capabilities.

The copyright videos shown on YouTube show that be changing several, straightforward parameters in your reactor you can drastically improve the agitation within the system.
Improvements can be made as simply as follows:

– Changing from an elongated reactor (sausage shape) to a squat reaction vessel
– Replacing anchor stirrers with four pitch paddles blades
– Via the addition of baffles

In the video clips below the following stands:

B = Baffles
A = Anchor agitator
U = Unbaffled
T = Turbine (four pitch paddle)
S = ‘Sausage shape’ (elongated reactor)

1. UT mixing time 180 rpm
Click here to watch

2. UT mixing beads 480 rpm
Click here to watch

3. UT extraction 500 rpm
Click here to watch

4. UA mixing time 180 rpm
Click here to watch

5. UA mixing beads 480 rpm
Click here to watch

6. ST mixing beads 480 rpm
Click here to watch

7. ST extraction 500 rpm
Click here to watch

8. SA mixing time 180 rpm
Click here to watch

9. Sa mixing beads 480 rpm
Click here to watch

10. BT mixing time 180 rpm_2
Click here to watch

11. BT extraction 500 rpm
Click here to watch

12. BA mixing time 180 rpm
Click here to watch

13. BA mixing beads 480 rpm
Click here to watch